3-甲基-3-丁烯-1-醇合成路线 (共 220 条)
反应条件
oxalic acid in water T=100°C; 4 h; oth. acid, oth. time; Product distribution;
参考文献
J. Appl. Chem. USSR (Engl. Transl.), , vol. 53, # 12 p. 2721 - 2726,2061 - 2065
反应条件
sulfuric acid T=25°C; acid-catalyzed isomerization, dehydratation and decomposition of isopentenols, retro-Prince reaction; Product distributionRate constant;
参考文献
Russian Chemical Bulletin, , vol. 43, # 2 p. 311 - 313
Izvestiya Akademi Nauk, Seriya Khimicheskaya, , # 2 p. 332 - 334
反应条件
trilithium phosphate T=230°C; activation energy; various temp.; Rate constantThermodynamic data;
参考文献
Russian Journal of Organic Chemistry, , vol. 33, # 7 p. 947 - 954
反应条件
sulfuric acid T=120°C; 3 h; various catalyst, various temperature, various time, extent of conversion, solvent cyclohexane; Product distribution;
参考文献
J. Appl. Chem. USSR (Engl. Transl.), , vol. 56, # 2 p. 333 - 337,316 - 319
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 227, p. 353
反应条件
1: 95 percent / NaN3 / dimethylformamide / 10 h / 20 °C 2: 65 percent / PPh3 / tetrahydrofuran; H2O / 20 h / 20 °C View Scheme
参考文献
Furman, Bartlomiej; Dziedzic, Magdalena
Tetrahedron Letters, 2003 , vol. 44, # 45 p. 8249 - 8252
反应条件
Oxonereg;; NH4Br in water; acetonitrile T=20°C; 0.0166667 h; regioselective reaction;
参考文献
Tetrahedron Letters, , vol. 53, # 11 p. 1401 - 1405
反应条件
Oxonereg;; NH4Br T=20°C; 0.5 h; regioselective reaction;
参考文献
Synthetic Communications, , vol. 43, # 23 p. 3121 - 3129
反应条件
Oxonereg;; NH4Br 2.3 h; Reflux; regioselective reaction;
参考文献
Synthetic Communications, , vol. 43, # 23 p. 3121 - 3129