Heinecke, Julie L.; Khin, Chosu; Pereira, Jose Clayston Melo; Suarez, Sebastian A.; Iretskii, Alexei V.; Doctorovich, Fabio; Ford, Peter C.
Journal of the American Chemical Society, 2013 , vol. 135, # 10 p. 4007 - 4017
Heinecke, Julie L.; Khin, Chosu; Pereira, Jose Clayston Melo; Suarez, Sebastian A.; Iretskii, Alexei V.; Doctorovich, Fabio; Ford, Peter C.
Journal of the American Chemical Society, 2013 , vol. 135, # 10 p. 4007 - 4017
sodium carbonate in neat (no solvent) byproducts: H2O, HCN; heating of sodium acetate, vigorous explosion; moderate reaction by addn. of equal amounts of Na2CO3 and NaNO2, vogorous flickering;;
sulfur dioxide; sodium carbonate; acetone in not given react. of SO2,Na2CO3 and NaNO2;adding acetone to the formed Na-hydroxylamine disulfonate at 70 °C;neutralization with NaOH; evapn.,recrystn. from water;
参考文献
Semon
Journal of the American Chemical Society, 1923 , vol. 45, p. 189
Full Text Show Details
Gmelin Handbook: N: MVol.4, 2.1, page 857 - 866
Full Text Show Details
Raschig, F.
Schwefel- und Stickstoffstudien, Leipzig-Berlin 1924,p.1
