T=40°C; entstehen noch Isopropylaether des 2.4-Diisopropyl-phenols und Isopropylaether des 2.4.6-Triisopropyl-phenols;
参考文献
Sowa; Hinton; Nieuwland
Journal of the American Chemical Society, 1932 , vol. 54, p. 3694,3695, 3697
Journal of the American Chemical Society, 1933 , vol. 55, p. 3402,5077
in dichloromethane (Ar), at -40/-50°C for 15-25 min; degassed (vac., -78°C), phases sepd., solid washed with CH2Cl2, exts. combined; not isolated, detected by NMR;
参考文献
Frohn; Franke; Fritzen; Bardin
Journal of Organometallic Chemistry, 2000 , vol. 598, # 1 p. 127 - 135
in chloroform-d1 BF3 and BCl3 passed through soln. of amine in dry CDCl3 at -50°C, excess of amine added or equilibrated mixt. of BF3 and BCl3 added to soln. of amine in dry CDCl3, frozen, degassed in vac.; without isolation;
参考文献
Fox, Arnold; Hartman, Stephen J.; Humphries, Robyn E.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1982 , p. 1275 - 1284
in dichloromethane (Ar), at -40/-50°C for 15-25 min; degassed (vac., -78°C), phases sepd., solid washed with CH2Cl2, exts. combined; not isolated, detected by NMR;
参考文献
Frohn; Franke; Fritzen; Bardin
Journal of Organometallic Chemistry, 2000 , vol. 598, # 1 p. 127 - 135
in gaseous matrix other Radiation; ac discharge in a mixt. of BF3, O2, and He (partial pressure of BF3, O2, and He 60, 290, and 750 mTorr, dry-ice temp.);; detd. by diode laser spectroscopy and by microwave spectroscopy;;
参考文献
Kawashima, Yoshiyuki; Kawaguchi, Kentarou; Endo, Yasuki; Hirota, Eizi
Journal of Chemical Physics, 1987 , vol. 87, # 4 p. 2006 - 2009
