all-cis-tetrakis[(diphenylphosphanyl)methyl]cyclopentane; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide T=130°C; 20 h; Title compound not separated from byproducts;
参考文献
European Journal of Organic Chemistry, , # 3 p. 765 - 774
potassium carbonate; Tedicyp; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide T=130°C; Heck reaction; 20 h; Title compound not separated from byproducts;
参考文献
Kondolff, Isabelle; Doucet, Henri; Santelli, Maurice
Synlett, 2004 , # 9 p. 1561 - 1564
1: With potassium carbonate; (dippp)2Pd in water T=130°C; Heck reaction; 1.5 h; microwave irradiation; 2: With hydrogenchloride in water; ethyl acetate T=20°C; Further stages.;
1: With 1,3-bis-(diphenylphosphino)propane; palladium diacetate; triethylamine in isopropyl alcohol T=115°C; Heck reaction; Inert atmosphere; 2: With hydrogenchloride; water in isopropyl alcohol 0.5 h;
参考文献
Hyder, Zeynab; Ruan, Jiwu; Xiao, Jianliang
Chemistry - A European Journal, 2008 , vol. 14, # 18 p. 5555 - 5566
