反应条件
in neat (no solvent) fusing tin and alkali metal chloride (sealed quartz ampule), grinding (N2 atmosphere over P2O5), gradual heating (quartz ampule, 110 - 130°C, 1 Pa), cooling (boiling N2 temp., vac., condensation of Cl2 to ampule), storing (4 - 8 d); opening, filling (He); detd. by Raman spectroscopy;
参考文献
Russian Journal of Inorganic Chemistry, , vol. 42, # 5 p. 631 - 632