in diethyl ether -70--20°C, then mixing at room temp.;
参考文献
Barbieri, G.; Taddei, F.
Journal of the Chemical Society [Section] B: Physical Organic, 1971 , p. 1903 - 1906
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.17, page 177 - 177
in ethanol; chloroform addn. of the metal halide in EtOH-CHCl3 to the org. ligand in EtOH-CHCl3 and heating for 150 min to 75-80°C; filtn., washing with water, EtOH-CHCl3 and Et2O, drying in a vac. desiccator (20 h at room temp., 6 h at 110°C); elem. anal.;
参考文献
Jalil, N. S. Neelam
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1989 , vol. 19, p. 1069 - 1084
in neat (no solvent) equimolar amt. of SnCl4 and Si-comp. were mixed, mixt. was stirred at 220 °C for 15 h, cooled in an ice-bath for 0.5 h, heated again at 220 °C for 1.5 h; distn. at 77 °C/0.025 Hgmm, elem. anal.;
参考文献
Aziz Choudhary; Mazhar; Salma; Ali; Qinglan; Molloy
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 2001 , vol. 31, # 2 p. 277 - 295
