反应条件
in diethyl ether; hexane
byproducts: LiCl; (N2); Schlenk technique or glovebox; soln. of Li compd. (2 equiv.) in Et2O was slowly added to soln. of SnCl4 (1 equiv.) in hexane at -78°C; soln. was warmed to room temp. and stirred for 5 h; filtered; solvents removed (vac.); oily residue filtered; distd. (vac.);filtered-off residue washed (hexane); dried (vac.); recrystd. (Et2O); e lem. anal.;
参考文献
Batsanov, Andrei S.; Cornet, Stephanie M.; Dillon, Keith B.; Goeta, Andres E.; Thompson, Amber L.; Xue, Bao Yu
Dalton Transactions, 2003 , # 12 p. 2496 - 2502
