in neat (no solvent) byproducts: C; from anhydrous ZnCl2 and CaC2 at 400°C;;
参考文献
Gelhaar, J.
Tek. Tidskr., 1932 , vol. 62, p. 81 - 86
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Gelhaar, J.
Chemiker-Zeitung, 1933 , vol. 57, p. 243 - 244
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Gmelin Handbook: Ca: MVol.B3, 88, page 843 - 845
in further solvent(s) Electrochem. Process; (N2), glove-box; Cu working electrode and Zn wire as reference electrodeimmersed in 50percent-50percent ZnCl2 - 1-ethyl-3-methyl imidazolium chloride, 120 °C; detd. by XRD;
参考文献
Lin, Yi-Wen; Tai, Chia-Cheng; Sun, I-Wen
Journal of the Electrochemical Society, 2007 , vol. 154, # 6 p. D316-D321
in neat (no solvent) byproducts: MgCl2; vac. or N2 filled glove box; mixt. grinding, heating in evac. sealed quartz ampoule at 850°C for 10 h, cooling to room temp., grinding; powder trituration with MeOH or H2O;
参考文献
Fitzmaurice, Jonathan C.; Hector, Andrew L.; Parkin, Ivan P.; Rowley , Adrian T.
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 101, # 1-4 p. 47 - 56