in hexane under Ar; 41 mmol ZnMes2 added to 82 mmol VOCl3 in hexane at -20°C; mixt. stirred at room temp. for 2-3 h; dark-blue ppt. (VOCl2*ZnCl2) filtered off; filtrate concd. and cooled; elem. anal.;
参考文献
Seidel, W.; Kreisel, G.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1988 , vol. 559, p. 118 - 122
water; oxygen in water attack of Zn with aq. soln. in presence of O2; with Zn, as bent stripe with two ends dipped into NaCl soln. (1percent, addn. of 2percent gelatine, trace of acetic acid and some drops phenole red), asymmetric accumulation of alkaline react. products;;
