Bernthsen
Justus Liebigs Annalen der Chemie, 1884 , vol. 224, p. 45
Full Text Show Details
Bernthsen; Bender
Chemische Berichte, 1883 , vol. 16, p. 1808
in neat (no solvent) High Pressure; pressure react. of dry HCl and Ph6Ge2 in autoclave (molar ratio HCl/Ph6Ge2 = 7.3), room temp., initial pressure 34 atm, 24h; rinsing react. mixt. with pentane into retort; evapn.; addn. of pentane; cooling to -15°C; crystn. overnight; filtration; recrystn. (petroleum ether); elem. anal.;
参考文献
Haeberle, Karl; Draeger, Martin
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1987 , vol. 42, # 3 p. 323 - 329