反应条件
in water addn. of aq. en into aq. soln. of Co complex, pH adjisted to 9 (HCl), heating and stirring (50°C, 2 h); vaolume reduction, repeated column chromy. (Sephadex G-10, SP-Sephadex C-25, aq. 0.2 M KCl), red band collected, volume reduction (vac.), addn. of MeOH, filtration off KCl; (sym-cis isomer obtained from purple-red band by same manner); elem. anal.;
参考文献
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, , vol. 29, # 9 p. 1567 - 1578
