反应条件
in N,N-dimethyl-formamide refluxing Mn-salt with porfyrin (2 h), cooling, extn. into CH2Cl2, washing (water), drying (Na2SO4), filtration, solvent removal (vac.), diisoln. in CH2Cl2, addn. of 10percent HCl sated. with NaCl; sepn. of org. layer, washing (water), drying (Na2SO4), chromy. (Al2O3, CH2Cl2, then CH2Cl2/MeOH=3:1 v/v), recrystn. (Me2CO/hexanes);
参考文献
Cheng, Beisong; Cukiernik, Fabio; Fries, Pascal H.; Marchon, Jean-Claude; Scheidt, W. Robert
Inorganic Chemistry, 1995 , vol. 34, p. 4627 - 4639