反应条件
1: 1.) LDA / 1.) THF, hexane, -10 deg C, 15 min, 2.) THF, hexane, -50 deg C, 6 h 2: Na2CO3 / H2O / 0.5 h / 0 °C 3: 97 percent / O2, methylene blue / methanol / 3 h / 0 °C / Irradiation 4: 1.) NaBH4, NaHCO3, 2.) acid / 1.) water, RT, 2 h, 2.) water, 1 h View Scheme
参考文献
Utaka, Masanori; Kuriki, Hidesuke; Sakai, Takashi; Takeda, Akira
Journal of Organic Chemistry, 1986 , vol. 51, # 6 p. 935 - 938
