1-苯基-2,2-二甲基环丙烷合成路线 (共 37 条)
反应条件
water; lithium in tetrahydrofuran
T=-78°C;
参考文献
Hoell,D.; Lex,J.; Muellen,K.
Journal of the American Chemical Society, 1986 , vol. 108, p. 5983
反应条件
oxygen; lithium in tetrahydrofuran
T=-78°C;
参考文献
Hoell,D.; Lex,J.; Muellen,K.
Journal of the American Chemical Society, 1986 , vol. 108, p. 5983
反应条件
BF3·2HOAc in dichloromethane
T=0°C;
参考文献
Fleming, Ian; Urch, Christopher J.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 173 - 192
反应条件
in dichloromethane
T=-78°C;
参考文献
Brookhart, M.; Humphrey, M. B.; Kratzer, H. J.; Nelson, G. O.
Journal of the American Chemical Society, 1980 , vol. 102, # 26 p. 7802 - 7803
反应条件
tetrafluoroboric acid in dichloromethane
T=-78°C;
参考文献
Kremer,K.A.; Kuo,G.H.; O'Connor,E.J.
Journal of the American Chemical Society, 1982 , vol. 104, p. 6119
反应条件
4-methoxy-toluene; iron(III) tris(dibenzoylmethane) in tetrahydrofuran
3 h; Ambient temperature;
参考文献
Nishii, Yoshinori; Wakasugi, Kazunori; Tanabe, Yoo
Synlett, 1998 , # 1 p. 66 - 69
反应条件
1: in tetrahydrofuran
T=-78 - 0°C;
2: With [VO(OEt)Cl2]
T=20°C; 5 h; Further stages.;
参考文献
Takada; Sakurai; Hirao
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 300 - 302
反应条件
bis(acetylacetonate)nickel(II); methyllithium in tetrahydrofuran; diethyl ether
T=65°C; 1 h;
参考文献
Gai, Yonghua; Julia, Marc; Verpeaux, Jean-Noel
Bulletin de la Societe Chimique de France, 1996 , vol. 133, # 9 p. 817 - 829
反应条件
lithium diethylamide in N,N,N',N',N'',N''-hexamethylphosphoric triamide; diethyl ether
T=0°C; 4 h;
参考文献
Babin, D.; Fourneron, J. D.; Harwood, L. M.; Julia, M.
Tetrahedron, 1981 , vol. 37, p. 325 - 332
反应条件
lithium; copper(II) bis(trifluoromethanesulfonate) in tetrahydrofuran
1) -78 deg C, 30 s, 2) RT, 45 min;
参考文献
Hoell,D.; Lex,J.; Muellen,K.
Journal of the American Chemical Society, 1986 , vol. 108, p. 5983