in water addn. of CsF to ZrO(NO3)2*2H2O soln. with stirring, homogenization of mixt. addn. of H3PO4 (5 wtpercent ZrO2; F/Zr molar ratio=3.8); pptn. for 7-45 ds, filtration, washing with H2O and EtOH, drying in air;elem. anal.;
参考文献
Godneva; Motov; Kuznetsov; Shchur
Russian Journal of Inorganic Chemistry, 2012 , vol. 57, # 4 p. 492 - 498