1-苯基-2-丙烯基-1-酮合成路线 (共 309 条)
参考文献
Kohler
American Chemical Journal, 1909 , vol. 42, p. 393
反应条件
1: ethyl-5-(2-hydroxyethyl)-4-methylthiazolium bromide, NEt3 / 2 h / 90 °C 2: TsOH / toluene / 100 °C View Scheme
参考文献
Perrier, Helene; Bayly, Christopher; Laliberte, France; Huang, Zheng; Rasori, Roberta; Robichaud, Annette; Girard, Yves; Macdonald, Dwight
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 3 p. 323 - 326
反应条件
palladium on activated charcoal in benzene 2 h; Heatingother time; other cond.: Et3N, 45 min, reflux; further α,β-unsaturated ketones; Product distribution;
参考文献
Nitta, Makoto; Iino, Yukio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , p. 435 - 440
反应条件
piperidine; bromine Kochen des Reaktionsprodukts mit Schwefelsaeure;
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 184, p. 99
Bulletin de la Societe Chimique de France, , vol. <4>41, p. 1375
反应条件
aufeinanderfolgend Einw. von Piperidin oder Diaethylamin und Kochen des Reaktionsprodukts mit Schwefelsaeure;
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 184, p. 99
Bulletin de la Societe Chimique de France, , vol. <4>41, p. 1375
反应条件
trifluorormethanesulfonic acid T=25°C; 120 h; further reagent: 6percent TFSA + 94percent TFA;
参考文献
Suzuki, Takayoshi; Ohwada, Tomohiko; Shudo, Koichi
Journal of the American Chemical Society, 1997 , vol. 119, # 29 p. 6774 - 6780
反应条件
HUSY-zeolite T=130°C; 15 h; sealed tube;
参考文献
Tetrahedron Letters, , vol. 48, # 33 p. 5911 - 5914
反应条件
RhH(CO)(triphenylphosphine)3 in methanol T=80°C; P=15001.2 Torr; 18 h;
参考文献
Sauthier, Mathieu; Castanet, Yves; Mortreux, Andre
Chemical Communications, 2004 , # 13 p. 1520 - 1521
反应条件
1: DABCO / tetrahydrofuran / Ambient temperature 2: 54 percent / benzene / 6 h / Irradiation View Scheme
参考文献
Allen; Bridgess
Journal of the American Chemical Society, 1929 , vol. 51, p. 2155
反应条件
methanol; [RhCl(η2:η2-cycloocta-1,5-diene)]2; triphenylphosphine T=80°C; P=15001.5 Torr; 18 h; AutoclaveInert atmosphere;
参考文献
Sauthier, Mathieu; Lamotte, Nicolas; Dheur, Julien; Castanet, Yves; Mortreux, Andre
New Journal of Chemistry, 2009 , vol. 33, # 5 p. 969 - 971