Le, Chichip Q.; Kunchithapatham, Kamala; Henderson, William H.; Check, Christopher T.; Stambuli, James P.
Chemistry - A European Journal, 2013 , vol. 19, # 34 p. 11153 - 11157
dichloro bis(acetonitrile) palladium(II); oxygen; copper dichloride in tetrahydrofuran T=25°C; P=760 Torr; 43 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
1.1: triethyl borane; trichlorosilane / tetrahydrofuran / 0 - 20 °C / In air 2.1: potassium fluoride; potassium hydrogencarbonate / tetrahydrofuran; methanol / 1 h / 20 °C / In air 2.2: 20 °C View Scheme
