2,2,6,6-四甲基哌啶合成路线 (共 107 条)
反应条件
in benzene T=146°C; 26 h; KineticsProduct distribution; Further Variations:TemperaturesSolventstime;
参考文献
Journal of Physical Organic Chemistry, , vol. 16, # 8 p. 559 - 563
反应条件
in acetonitrile Ambient temperatureIrradiationin isooctane; Product distributionRate constantMechanism;
参考文献
Journal of Organic Chemistry, , vol. 49, # 26 p. 5214 - 5217
反应条件
in water Rate constant;
参考文献
Journal of Pharmaceutical Sciences, , vol. 81, # 7 p. 652 - 656
反应条件
in decane T=150°C; Oxidation; 2.5 h; Product distributionKinetics;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 7 p. 1363 - 1367
反应条件
in hexane Product distribution;
参考文献
Chemische Berichte, , vol. 118, # 9 p. 3759 - 3770
反应条件
hydrogenchloride; n-butyllithium; sodium sulfate in tetrahydrofuran; hexane; N,N-dimethyl-formamide
参考文献
Clariant GmbH
Patent: US2001/50352 A1, 2001 ;
反应条件
n-butyllithium in tetrahydrofuran 1 h;
参考文献
YAMANOUCHI PHARMACEUTICAL CO. LTD.
Patent: EP1184376 A1, 2002 ;
Location in patent: Page 12 ;
反应条件
in tetrahydrofuran T=30°C; Equilibrium constant;
参考文献
Ahlbrecht, Hubertus; Schneider, Gunther
Tetrahedron, 1986 , vol. 42, # 17 p. 4729 - 4742
反应条件
1: 2,2,6,6-tetramethyl-piperidine With sodium hydride in toluene T=20°C; 0.166667 h; 2: 4-methoxy-benzoyl chloride in toluene 24 h; Heating;
参考文献
Clayden, Jonathan; Foricher, Yann J. Y.; Lam, Ho Kam
European Journal of Organic Chemistry, 2002 , # 21 p. 3558 - 3565
反应条件
in dichloromethane T=20°C; 2 h; Inert atmosphere;
参考文献
European Journal of Inorganic Chemistry, , # 25 p. 3967 - 3975