反应条件
methylamine in water A concd. soln. of KI is added to a soln. of K2PtCl4, mixt. is stirred for 20 min, soln. is filtered with stirring into a dilute aq. soln. of the ligand.; Pptn., if the ppt. contained a trace of brown, stirring for 30-40 min, yellow ppt. is filtered off, washed with water, ethanol and ether, and dried in vac., recrystn. from DMF/water at room temp.;
参考文献
Souchard, Jean-Pierre; Wimmer, Franz L.; Ha, Tam T. B.; Johnson, Neil P.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1990 , # 1 p. 307 - 310