反应条件
in tetrahydrofuran
under N2, dried solvent; at -60°C addn. of the W-compd. to a soln. of an equimol. amt. alkali salt in THF (prepd. by scission of BiPh2Cl with Na in liq. NH3), stirring for 1 h; removal of solvent at -30°C in vac., sepn. of the W-compd. by chromy. (silica gel, pentane/CH2Cl2), recrystn. from CH2Cl2/pentane, sepn. of the Bi-compd. by chromy. (CH2Cl2/ether), recrystn. from CH2Cl2; elem. anal.;
参考文献
Fischer, Ernst Otto; Reitmeier, Rudolf
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1983 , vol. 38, # 5 p. 582 - 586