1,3-二甲基巴比妥酸合成路线 （共 143 条）
反应条件
pyridine in dichloromethane
参考文献
JOHNS HOPKINS UNIVERSITY; GUTHRIE, Daryl A.
Patent: WO2013/59194 A1, 2013 ;
Location in patent: Page/Page column 38 ;
反应条件
trichlorophosphate
T=120°C;
参考文献
Siddiqui, Zeba N.; Mohammed Musthafa; Ahmad, Anis; Khan, Asad U.
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 10 p. 2860 - 2865
反应条件
1: 76 percent / Et3N / methanol / 4 h / 80 - 85 °C
2: 68 percent / (NH4)2CO3, AcOH / 8 h / Heating
View Scheme
参考文献
Zoorob, Hanafi H.; Abou-El Zahab, Mohamed M.; Abdel-Mogib, Mamdouh; Ismail, Mohamed A.
Tetrahedron, 1996 , vol. 52, # 30 p. 10147 - 10158
反应条件
1: POCl3
2: N2H4+H2O
3: NaNO2; aqueous HCl
View Scheme
参考文献
Pfleiderer; Schuendehuette
Justus Liebigs Annalen der Chemie, 1958 , vol. 612, p. 158,162
反应条件
T=120°C; 0.333333 h;
参考文献
Deb, Mohit L.; Bhuyan, Pulak J.
Tetrahedron Letters, 2007 , vol. 48, # 12 p. 2159 - 2163
参考文献
Deb, Mohit L.; Bhuyan, Pulak J.
Tetrahedron Letters, 2007 , vol. 48, # 12 p. 2159 - 2163
反应条件
1: sodium iodide / methanol / 20 °C / |Electrolysis
2: hydrogenchloride / water / 1 h
View Scheme
参考文献
Vereshchagin, Anatoly N.; Elinson, Michail N.; Dorofeeva, Evgeniya O.; Gorbunov, Sergey V.; Belyakov, Pavel A.; Chizhov, Alexander O.; Nikishin, Gennady I.; Bushmarinov, Ivan S.
Journal of Molecular Catalysis A: Chemical, 2012 , vol. 363-364, p. 69 - 73,5
参考文献
Bredereck; Pfleiderer
Chemische Berichte, 1954 , vol. 87, p. 1268,1273
Full Text Show Details
Burroughs Wellcome and Co.
Patent: US2581889 , 1949 ;
反应条件
in water
T=20°C; Knoevenagel condensation; 0.0833333 h;
参考文献
Deb, Mohit L.; Bhuyan, Pulak J.
Tetrahedron Letters, 2005 , vol. 46, # 38 p. 6453 - 6456
反应条件
bromocyane; L-(+)-tartaric acid in methanol
T=0 - 20°C; screw cap tube;
参考文献
Jalilzadeh, Mohammad; Pesyan, Nader Noroozi
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 9 p. 3382 - 3388
