3-(2-氨基乙基)苯胺合成路线 (共 14 条)
反应条件
palladium 10 on activated carbon; hydrogen in isopropyl alcohol T=20°C; 24 h; Inert atmosphere;
参考文献
Pesnot, Thomas; Gershater, Markus C.; Ward, John M.; Hailes, Helen C.
Chemical Communications, 2011 , vol. 47, # 11 p. 3242 - 3244
反应条件
trifluoroacetic acid T=20°C; 0.5 h;
参考文献
EP2168966 A1, ;
Page/Page column 61 ;
EP 2168966 A1
反应条件
tin(ll) chloride in ethanol T=70°C;
参考文献
Journal of Medicinal Chemistry, , vol. 46, # 9 p. 1661 - 1669
反应条件
1.1: BH3 / tetrahydrofuran / 25 °C 1.2: aq. HCl / tetrahydrofuran / 0 °C 2.1: SnCl2*2H2O / ethanol / 70 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 46, # 9 p. 1661 - 1669
反应条件
hydrogen azide; sulfuric acid
参考文献
Journal of the American Chemical Society, , vol. 71, p. 2137,2138,2140
反应条件
1: Raney nickel; water / 50 °C / Hydrogenation.anschliessend Hydrierung an Platin in Aethanol; anschliessende Behandlung mit Benzoylchlorid 2: hydrazoic acid; sulfuric acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 71, p. 2137,2138,2140
反应条件
sulfuric acid; palladium; acetic acid Hydrogenation;
参考文献
Chemische Berichte, , vol. 68, p. 1579,1581
反应条件
1: triethylamine 2: lead (II)-acetate; aq.-ethanolic hydrochloric acid; acetic acid / Electrolysis.an einer Quecksilber-Kathode View Scheme
参考文献
Chemische Berichte, , vol. 68, p. 184,187
反应条件
1: sodium hypochlorite / 60 - 70 °C 2: tin (II)-chloride; concentrated hydrochloric acid; glacial acetic acid View Scheme
参考文献
Journal of the Chemical Society, , p. 1674
参考文献
Chemische Berichte, , vol. 68, p. 1579,1581