1,3-二溴-5,5-二甲基海因合成路线 (共 64 条)
参考文献
ALBEMARLE CORPORATION
Patent: EP1250045 B1, 2003 ;
反应条件
sodium hydroxide; bromine; sodium carbonate
反应条件
water anschliessend mit wss.NaOH und Brom;
参考文献
Anales de la Asociacion Quimica Argentina (1921-2001), , vol. 41, p. 153
反应条件
in dichloromethane T=20°C; 1 h; Overall yield = 97 percent; Overall yield = 398 mg;
参考文献
Hu, Jian-Yong; Feng, Xing; Seto, Nobuyuki; Do, Jung-Hee; Zeng, Xi; Tao, Zhu; Yamato, Takehiko
Journal of Molecular Structure, 2013 , vol. 1035, p. 19 - 26
反应条件
T=25°C; Rate constant;
参考文献
Orazi; Corral
Anales de la Asociacion Quimica Argentina (1921-2001), 1954 , vol. 42, p. 139,145
反应条件
1: pyrene; 1,3-dibromo-5,5-dimethyl-hydantoin in dichloromethane T=20°C; 1 h; 2: 4,4'-dimethyldiphenylamine With tri-tert-butyl phosphine; palladium diacetate; caesium carbonate in o-xylene T=120°C; Buchwald-Hartwig Coupling; 48 h; Overall yield = 73 percent;
参考文献
Hu, Jian-Yong; Feng, Xing; Seto, Nobuyuki; Do, Jung-Hee; Zeng, Xi; Tao, Zhu; Yamato, Takehiko
Journal of Molecular Structure, 2013 , vol. 1035, p. 19 - 26
反应条件
in water; ethyl acetate; isopropyl alcohol
参考文献
FUJIFILM CORPORATION
Patent: US2012/76950 A1, 2012 ;
参考文献
Orazi; Salellas
Anales de la Asociacion Quimica Argentina (1921-2001), 1950 , vol. 38, p. 188,191
参考文献
Anales de la Asociacion Quimica Argentina (1921-2001), , vol. 38, p. 5,9
参考文献
Anales de la Asociacion Quimica Argentina (1921-2001), , vol. 40, p. 91,97
Anales de la Asociacion Quimica Argentina (1921-2001), , vol. 37, p. 263,266
Anales de la Asociacion Quimica Argentina (1921-2001), , vol. 38, p. 5,10
Anales de la Asociacion Quimica Argentina (1921-2001), , vol. 38, p. 5,9