3-甲基-3-苯基缩水甘油酸乙酯合成路线 (共 10 条)
反应条件
potassium n-butoxide
参考文献
McCarthy, Daniel G.; Hegarty, Anthony F.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 579 - 591
反应条件
1: With samarium diiodide in tetrahydrofuran T=20°C; 2 h; 2: With potassium hexamethyl-disilazane in tetrahydrofuran; toluene
参考文献
Concellon, Jose M.; Concellon, Carmen; Diaz, Pamela
European Journal of Organic Chemistry, 2006 , # 9 p. 2197 - 2200
反应条件
methyltrioxorhenium (VII) T=50 - 60°C; 72 h;
参考文献
Zhu, Zuolin; Espenson, James H.
Journal of the American Chemical Society, 1996 , vol. 118, # 41 p. 9901 - 9907
反应条件
1: 86 percent / zinc chloride/silver acetate/bronze-coloured C8K / tetrahydrofuran / 0.33 h / -78 °C 2: 80 percent / K2CO3 View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 336, p. C33 - C36
参考文献
Fuerstner, Alois
Journal of Organometallic Chemistry, 1987 , vol. 336, p. C33 - C36
反应条件
2: acidic permanganate View Scheme
参考文献
McCarthy, Daniel G.; Hegarty, Anthony F.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 579 - 591
反应条件
2: acidic permanganate 3: thionyl chloride View Scheme
参考文献
McCarthy, Daniel G.; Hegarty, Anthony F.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 579 - 591
反应条件
1: 1.) NaN3, conc. H2SO4, 2.) SOCl2, Et3N / 1.) DMSO, 90 deg C, 2 h, 2.) CH2Cl2, RT, 4 h 2: 74 percent / xylene / 0.83 h / Heating View Scheme
参考文献
Murakami, Yasuoki; Watanabe, Toshiko; Suzuki, Hideharu; Kotake, Nobuyo; Takahashi, Tomoko; Toyonari, Kiyono; Ohno, Masami; Takase, Kyoko; Suzuki, Takayuki; Kondo, Kazuhiro
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 11 p. 1739 - 1744
反应条件
1: sodium; ethanol
2: acetic acid anhydride
View Scheme
参考文献
Pfau; Plattner
Helvetica Chimica Acta, 1932 , vol. 15, p. 1250,1265
反应条件
1: aqueous NaOH / Erhitzen des Reaktionsprodukts auf 180grad unter Durchleiten von Wasserdampf
View Scheme
参考文献
Newman; Closson
Journal of the American Chemical Society, 1944 , vol. 66, p. 1553