1.1: boron trifluoride diethyl etherate / 3 h / 120 °C
2.1: lithium hexamethyldisilazane / tetrahydrofuran / 3 h / -78 - -10 °C
2.2: -78 - 20 °C
3.1: acetic acid; sulfuric acid / 3.5 h / 95 - 100 °C
4.1: lithium hydroxide hydrate / tetrahydrofuran / 2 h / 20 °C
View Scheme
参考文献
Martin-Benlloch, Xavier; Elhabiri, Mourad; Lanfranchi, Don Antoine; Davioud-Charvet, Elisabeth
Organic Process Research and Development, 2014 , vol. 18, # 5 p. 613 - 617
