反应条件
in benzene byproducts: FeCl2; under anhyd. conditions and an atmosphere of dry N2; slow addn. with continuous stirring of the Sb-compd. in benzene to the Fe-compd. in benzene, passing the N2 gas for 24 h with occasional shaking; filtering off the FeCl2 and evapn. of the filtrate, recrystn. of the crude residue from benzene;
参考文献
Sharma, Hemant K.; Singh, Soran; Dubey, S. N..; Puri, D. M.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1982 , vol. 21, # 6 p. 619 - 621
