2,3,4,5,6-五氟苯胺合成路线 (共 126 条)
反应条件
in hexane T=20°C; 6 h; Irradiation; Product distribution;
参考文献
Journal of Fluorine Chemistry, , vol. 28, p. 23
反应条件
(1,1'-biphenyl)-4-ylphenylmethanone T=25°C; Irradiationvariation of temperature; without sensitizer; Product distribution;
参考文献
Tetrahedron Letters, , vol. 30, # 1717 p. 2199 - 2202
反应条件
in dimethyl sulfoxide T=25°C; Equilibrium constant;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 25, # 11.1 p. 2041 - 2044
Zhurnal Organicheskoi Khimii, , vol. 25, # 11 p. 2261 - 2265
反应条件
in dimethyl sulfoxide T=25°C; Equilibrium constant;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 25, # 11.1 p. 2041 - 2044
Zhurnal Organicheskoi Khimii, , vol. 25, # 11 p. 2261 - 2265
反应条件
[Cu(I)(CH3CN)4]PF6; dimethylphenylsilane; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene 12 h; Inert atmosphereReflux; Catalytic behavior; SolventReagent/catalyst; regioselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 11 p. 3203 - 3207
Angew. Chem., , vol. 125, # 11 p. 3285 - 3289,5
反应条件
Ambient temperatureIrradiationother solvents and additives, var. temp., photolysis time, also photosensitizer; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 114, # 13 p. 5054 - 5067
参考文献
Chemistry and Industry (London, United Kingdom), , p. 630
Journal of the Chemical Society, , p. 1768,1770
反应条件
in N,N-dimethyl-formamide; chlorobenzene 1.) 90 deg C, 1 h, 2.) 80 deg C, 3 h;
参考文献
Barton; Fontana; Yang
Tetrahedron, 1996 , vol. 52, # 8 p. 2705 - 2716
反应条件
1.1: |Reflux 2.1: zinc; [NiCl2(py)4] / 1-methyl-pyrrolidin-2-one; water / 4 h / 70 °C / |Inert atmosphere 2.2: 1 h / 20 °C View Scheme
参考文献
Prikhodko; Adonin; Parmon
Russian Chemical Bulletin, 2009 , vol. 58, # 11 p. 2304 - 2310
Izv. Akad. Nauk, Ser. Khim., 2009 , # 11 p. 2234 - 2239,6
反应条件
1: With [Pd(dppe)(H2O)2](TfO)2 in 1,4-dioxane T=80°C; 18 h; 2: With silica gel in dichloromethane T=20°C; 2 h;
参考文献
European Journal of Organic Chemistry, , # 1 p. 59 - 62