(S)-1-苯基-3-丁烯-1-醇合成路线 （共 84 条）
反应条件
in diethyl ether
T=-78°C;
参考文献
Bressy, Cyril; Allais, Florent; Cossy, Janine
Synlett, 2006 , # 20 p. 3455 - 3456
反应条件
diisobutylaluminium hydride in tetrahydrofuran; hexane
12 h; Reflux;
参考文献
Lange, Heiko; Huenerbein, Robert; Wibbeling, Birgit; Froehlich, Roland; Grimme, Stefan; Hoppe, Dieter
Synthesis, 2008 , # 18 art. no. T06008SS, p. 2905 - 2918
反应条件
4 A molecular sieve; oxygen
1.) toluene, -78 deg C, 2.) hν, CH3CN; Yield given. Multistep reaction;
参考文献
Roush, William R.; Park, Jae Chan
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1143 - 1144
反应条件
sodium tetrahydroborate; 4 A molecular sieve
1.) toluene, -78 deg C, 2.) -78 deg C, EtOH; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Roush, William R.; Hoong, Lee K.; Palmer, Michelle A. J.; Park, Jae Chan
Journal of Organic Chemistry, 1990 , vol. 55, # 13 p. 4109 - 4117
反应条件
tetrabutyl ammonium fluoride
Yield given;
参考文献
Yu, Chan-Mo; Choi, Ha-Soon; Jung, Won-Hyuk; Lee, Sung-Soo
Tetrahedron Letters, 1996 , vol. 37, # 39 p. 7095 - 7098
反应条件
sodium tetrahydroborate; 4 A molecular sieve
1.) THF, -78 deg C, 2.) EtOH, -78 deg C; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Roush, William R.; Hoong, Lee K.; Palmer, Michelle A. J.; Park, Jae Chan
Journal of Organic Chemistry, 1990 , vol. 55, # 13 p. 4109 - 4117
反应条件
titanium tetrachloride in dichloromethane
T=-50°C; 22 h; the ee was investigated; Product distribution;
参考文献
Chan, T.H.; Wang, D.
Tetrahedron Letters, 1989 , vol. 30, # 23 p. 3041 - 3044
反应条件
4 A molecular sieve; scandium tris(trifluoromethanesulfonate) in dichloromethane
T=-78°C; 2 h; Product distribution; Further Variations:ReagentsSolventsTemperatures;
参考文献
Gravel, Michel; Lachance, Hugo; Lu, Xiaosong; Hall, Dennis G.
Synthesis, 2004 , # 8 p. 1290 - 1302
反应条件
acetoxytrimethylsilane; boron trifluoride diethyl etherate in cyclohexane
Prins cyclization; optical yield given as percent eestereoselective reaction;
参考文献
Parker, Gregory D.; Seden, Peter T.; Willis, Christine L.
Tetrahedron Letters, 2009 , vol. 50, # 26 p. 3686 - 3689
参考文献
Bates, Roderick W.; Aslam, Nur Filza Bte Mohamed; Tang, Chi H.; Simon, Oliver
Tetrahedron, 2014 , vol. 70, # 12 p. 2134 - 2140
