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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
77152-08-0
合成路线
（共 108 条）
1120-90-7
3-碘吡啶
+
77152-08-0
→
反应条件
3796-23-4
3-三氟甲基吡啶
反应条件
triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide T=23 - 50°C; 48 h; GloveboxSealed tube;
参考文献
Lishchynskyi, Anton; Novikov, Maxim A.; Martin, Eddy; Escudero-Adan, Eduardo C.; Novak, Petr; Grushin, Vladimir V.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11126 - 11146
626-55-1
3-溴吡啶
+
77152-08-0
→
反应条件
3796-23-4
3-三氟甲基吡啶
反应条件
triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide T=23 - 60°C; 15 h; GloveboxSealed tube;
参考文献
Lishchynskyi, Anton; Novikov, Maxim A.; Martin, Eddy; Escudero-Adan, Eduardo C.; Novak, Petr; Grushin, Vladimir V.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11126 - 11146
77152-08-0
+
1692-25-7
吡啶-3-硼酸
→
反应条件
3796-23-4
3-三氟甲基吡啶
反应条件
triethyl amine hydrochloride in N,N-dimethyl-formamide T=20°C; 4 h;
参考文献
Serizawa, Hiroki; Aikawa, Kohsuke; Mikami, Koichi
Chemistry - A European Journal, 2013 , vol. 19, # 52 p. 17692 - 17697
589-87-7
对溴碘苯
+
77152-08-0
→
反应条件
402-43-7
对溴三氟甲苯
反应条件
triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide T=23 - 50°C; 42 h; GloveboxSealed tube;
参考文献
Lishchynskyi, Anton; Novikov, Maxim A.; Martin, Eddy; Escudero-Adan, Eduardo C.; Novak, Petr; Grushin, Vladimir V.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11126 - 11146
577-19-5
1-溴-2-硝基苯
+
77152-08-0
→
反应条件
384-22-5
2-硝基-Alpha,Alpha,Alpha-三氟甲苯
反应条件
triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide T=23 - 50°C; 18 h; Inert atmosphere;
参考文献
Lishchynskyi, Anton; Novikov, Maxim A.; Martin, Eddy; Escudero-Adan, Eduardo C.; Novak, Petr; Grushin, Vladimir V.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11126 - 11146
696-62-8
4-碘苯甲醚
+
77152-08-0
→
反应条件
402-52-8
4-三氟甲基苯甲醚
反应条件
triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide T=23 - 50°C; 48 h; Inert atmosphere; TemperatureTime;
参考文献
Lishchynskyi, Anton; Novikov, Maxim A.; Martin, Eddy; Escudero-Adan, Eduardo C.; Novak, Petr; Grushin, Vladimir V.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11126 - 11146
5720-07-0
4-甲氧基苯硼酸
+
77152-08-0
→
反应条件
402-52-8
4-三氟甲基苯甲醚
反应条件
triethyl amine hydrochloride in N,N-dimethyl-formamide; toluene T=20°C; 1 h;
参考文献
Serizawa, Hiroki; Aikawa, Kohsuke; Mikami, Koichi
Chemistry - A European Journal, 2013 , vol. 19, # 52 p. 17692 - 17697
17933-03-8
3-甲基苯硼酸
+
77152-08-0
→
反应条件
401-79-6
3-甲基三氟甲苯
反应条件
oxygen; triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide T=25°C; 3.5 h;
参考文献
Novak, Petr; Lishchynskyi, Anton; Grushin, Vladimir V.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 31 p. 7767 - 7770
625-95-6
3-碘甲苯
+
77152-08-0
→
反应条件
401-79-6
3-甲基三氟甲苯
反应条件
triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide T=23 - 50°C; 48 h; GloveboxSealed tube; Time;
参考文献
Lishchynskyi, Anton; Novikov, Maxim A.; Martin, Eddy; Escudero-Adan, Eduardo C.; Novak, Petr; Grushin, Vladimir V.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11126 - 11146
77152-08-0
+
156545-07-2
3,5-二氟苯硼酸
→
反应条件
401-85-4
3,5-二氟三氟甲苯
反应条件
oxygen; triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide; toluene T=25°C; 2 h;
参考文献
Novak, Petr; Lishchynskyi, Anton; Grushin, Vladimir V.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 31 p. 7767 - 7770
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