antimony pentachloride in neat (no solvent) slow addn. of SbF3 to a mixture of SOCl2 and SbCl5 at 50 °C and 200 Torr; apparatus described;; fractionation; condensation;;
in neat (no solvent) dropping IF5 to SOCl2 at room temp.;; condensation (cooling by liquid air); removal of ICl3 and Cl2 by Hg (shaking); fractionation;;
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Gmelin Handbook: S: MVol.B3, 157, page 1863 - 1864
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Jonas, H.
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Yu, Wei-Lun; Jones, Brian D.; Kang, Minjin; Hammons, Justin C.; La Clair, James J.; Burkart, Michael D.
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