反应条件
in not given dropwise addn. of thionyl chloride to tetraalkyltin(IV) compd. under dry N2 atmosphere under ice cooling, warming to room temp., refluxing for 30 min; distn. (removal of excess of SOCl2), cooling resulting liquids, sepn., elem. anal.;
参考文献
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical, , vol. 22, # 3 p. 246 - 247
