in neat (no solvent) To silane-compd. freshly distd. PCl3 was dropwise added, mixt. was heated to 30-40°C.; The silane-compd. is distd. off.;
参考文献
Krolevets, A. A.; Martynov, I. V.
Journal of General Chemistry USSR (English Translation), 1991 , vol. 61, p. 236 - 236
Zhurnal Obshchei Khimii, 1991 , vol. 61, p. 259 - 259