反应条件
in hexane byproducts: (C6H5CH2)2S, C6H5CH2Br, C6H5CH2SH; Ti complex suspended in hexanes, addn. of Br2, stirred (15 min.), purple slurry immediately becoming brown; ppt. collected on a filter in air, dried (Cp2TiBr2 in high yield); removal of solvent from the filtrate (mostly disulfide, minute amts. of the monosulfides and bromide, GC anal.);
参考文献
Shaver, Alan; Morris, Stephen; Desjardin, Alain
Inorganica Chimica Acta, 1989 , vol. 161, p. 11 - 12