trimethylstannyl chloride in carbon disulfide under N2, reaction of P4 with Br2 in CS2, followed by treatment with C(CH3)3SnCl; further products: PBr3, PClBr2, PCl2Br, PCl3, P7Br3, P4Br2, and P4BrCl; not isolated, identified by 31P-NMR spectroscopy;
参考文献
Tattershall, Bruce W.; Kendall, Nigel L.
Polyhedron, 1994 , vol. 13, p. 1517 - 1522
in carbon disulfide under N2, dropwise addn. of Br2/CS2 to a stirred soln. of P4/CS2 (-10°C, 1 h), yellow soln.; not isolated, identified by 31P-NMR spectroscopy, molar ratio of PBr3, P2Br4, exo,exo-P4Br2 and exo,endo-P4Br2: 95 : 2.7 : 0.48 : 1.9;
参考文献
Tattershall, Bruce W.; Kendall, Nigel L.
Polyhedron, 1994 , vol. 13, p. 1517 - 1522
Suter; Zook
Journal of the American Chemical Society, 1944 , vol. 66, p. 741
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Read; Reid
Journal of the Chemical Society, 1928 , p. 1489
