in neat (no solvent) The halogen was co-condensed in a flask at -196°C with the mixt. of SiF4 and SiF2 emerging out of the reactor tube; further products;; warmed to room temp.; the volatile products were sepd. and detected by NMR and MS;;
参考文献
Suresh, Bettadapura S.; Thompson, James Charlton
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1987 , p. 1123 - 1126
in neat (no solvent) heating of a mixture of Si2F6 and an excess of Br2; inflammation;;
参考文献
Schumb, W. C.; Anderson, H. C.
Journal of the American Chemical Society, 1936 , vol. 58, p. 994 - 996
Full Text View citing articles Show Details
Gmelin Handbook: Si: MVol.B, 271, page 730 - 732
in neat (no solvent) The halogen was co-condensed in a flask at -196°C with the mixt. of SiF4 and SiF2 emerging out of the reactor tube; further products;; warmed to room temp.; the volatile products were sepd. and detected by NMR and MS;;
参考文献
Suresh, Bettadapura S.; Thompson, James Charlton
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1987 , p. 1123 - 1126
in dichloromethane addn. of bromine to a suspn. of SbPh2F at -97°C, warming to -40°C; evapn., cooling to -97°C, crystn., fractional crystn. of the mother liquor, elem. anal.;
参考文献
Bone, Stephen P.; Begley, Michael J.; Sowerby, D. Bryan
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1992 , # 13 p. 2085 - 2092
