反应条件
in pentane Under protective gas; pentane solns. of trineopentylaluminum and AlBr3 are combined in an evacuated tube, refluxing (30 min, 60°C oil bath).; Evapn., distn. (short-path) or recrystn. from small vol. of pentane at -78°C, elem. anal., mol wt.;
参考文献
Beachley, O. T. Jr.; Victoriano, L.
Organometallics, 1988 , vol. 7, p. 63 - 67
