三氯一氧化钒 三氯代氧化钒(V)合成路线 （共 117 条）
反应条件
sugar coal in neat (no solvent)
参考文献
Roscoe, H. E.
Justus Liebigs Annalen der Chemie, 1868 , vol. 6, p. 77 - 116
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Roscoe, H. E.
Philosophical Transactions of the Royal Society of London, 1868 , vol. 158, p. 1 - 27
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Roscoe, H. E.
Justus Liebigs Annalen der Chemie, 1870 , vol. 7, p. 70 - 87
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Roscoe, H. E.
Philosophical Transactions of the Royal Society of London, 1869 , vol. 159, p. 679 - 692
反应条件
hydrogen in neat (no solvent) byproducts: V-oxide chlorides;
参考文献
Roscoe, H. E.
Justus Liebigs Annalen der Chemie, 1868 , vol. 6, p. 77 - 116
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Roscoe, H. E.
Philosophical Transactions of the Royal Society of London, 1868 , vol. 158, p. 1 - 27
反应条件
hydrogen; carbon in neat (no solvent) byproducts: V-oxide chlorides;
参考文献
Roscoe, H. E.
Justus Liebigs Annalen der Chemie, 1868 , vol. 6, p. 77 - 116
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Roscoe, H. E.
Philosophical Transactions of the Royal Society of London, 1868 , vol. 158, p. 1 - 27
反应条件
hydrogen in neat (no solvent) at 500 - 850°C;;
参考文献
McCarley, R. E.; Roddy, J. W.
Journal of Inorganic and Nuclear Chemistry, 1960 , vol. 15, p. 293 - 296
反应条件
N2H5Cl in tetrachloromethane heating 10 - 15 h under N2 at reflux;; heating with CS2; pptn. washing with CHCl3 and ether;;
参考文献
Gmelin Handbook: V: MVol.B1, 76, page 207 - 210
反应条件
disulfur dichloride; chlorine in neat (no solvent) at 610°C; cooling down at ambiente temp.;; heating 10 min at 200°C;;
参考文献
Gmelin Handbook: S: MVol.A3, 5.3.4, page 713 - 718
反应条件
in neat (no solvent) at 150°C;;
参考文献
Brown, F. E.; Griffitts, F. A.
Iowa State College Journal of Science, 1934 , vol. 9, p. 89 - 93
反应条件
disulfur dichloride in neat (no solvent) heating under reflux at 145 - 150°C;; distillation of excess of S2Cl2; removing of excess of S on heating in CO2-stream or in vacuum at 300°C;;
参考文献
Emeleus, H. J.; Gutmann, V.
Journal of the Chemical Society, 1949 , p. 2979 - 2982
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Ruff, O.; Lickfett, H.
Ber. Dtsch. Chem. Ges., 1911 , vol. 44, p. 506 - 521
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Gmelin Handbook: V: MVol.B1, 75, page 205 - 207
反应条件
hydrogen in neat (no solvent) at 500 - 850°C;;
参考文献
McCarley, R. E.; Roddy, J. W.
Journal of Inorganic and Nuclear Chemistry, 1960 , vol. 15, p. 293 - 296
反应条件
in cyclohexane under N2;; not isolated;;
参考文献
Gmelin Handbook: V: MVol.B1, 91, page 246 - 247
