2,4,6-三甲基苯磺酰氯合成路线 (共 56 条)
反应条件
aluminium trichloride
参考文献
Horner,L.; Meyer,E.
Justus Liebigs Annalen der Chemie, 1975 , p. 2053 - 2078
反应条件
sodium hydroxide in dichloromethane 16 h; Ambient temperature;
参考文献
Bergeron, Raymond J.; McManis, James S.; Liu, Charles Z.; Feng, Yang; Weimar, William R.; et al.
Journal of Medicinal Chemistry, 1994 , vol. 37, # 21 p. 3464 - 3476
反应条件
pyridine in dichloromethane 1.5 h; Heating;
参考文献
McConnaughie; Jenkins
Journal of Medicinal Chemistry, 1995 , vol. 38, # 18 p. 3488 - 3501
反应条件
N-ethyl-N,N-diisopropylamine in tetrahydrofuran
参考文献
Patel, Dinesh; Jacobs, Jeffrey W.; Jain, Rakesh; Ni, Zhi-Jie; Yuan, Zhengyu
Patent: US2002/115863 A1, 2002 ;
参考文献
Nakamura, Hiroshi; Yoshida, Tsukasa; Todoko, Masaaki; Ueno, Keihei; Takagi, Makoto
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 10 p. 2839 - 2846
反应条件
hydrazine in dichloromethane 0.25 h;
参考文献
Yang, Fu-Lai; Ma, Xian-Tao; Tian, Shi-Kai
Chemistry - A European Journal, 2012 , vol. 18, # 6 p. 1582 - 1585
反应条件
lithium aluminium tetrahydride in diethyl ether 5 h; Heating;
参考文献
Blower, Philip J.; Dilworth, Jonathan R.; Hutchinson, John P.; Zubieta, Jon A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1985 , p. 1533 - 1542
反应条件
samarium; potassium iodide; nickel dichloride in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=60°C;
参考文献
Zhan, Zhuangping; Guo, Hongyun; Zhang, Yongmin
Synthetic Communications, 1997 , vol. 27, # 16 p. 2749 - 2752
反应条件
hydrogenchloride; acetic acid; triethylamine in tetrahydrofuran; chloroform; benzene
参考文献
Miles Laboratories, Inc.
Patent: US4159998 A1, 1979 ;
反应条件
triethylamine in dichloromethane
T=25°C; 24 h;
参考文献
Suwinski, Jerzy; Salwinska, Ewa
Tetrahedron, 1994 , vol. 50, # 19 p. 5741 - 5752