2,4,6-三甲基苯磺酰氯合成路线 （共 56 条）
反应条件
sodium hydroxide in water; toluene
参考文献
NIPPON KAYAKU KABUSHIKI KAISHA
Patent: EP361232 A3, 1991 ;
反应条件
triethylamine in 1,4-dioxane
1 h; Ambient temperature;
参考文献
Ohtsuka, E.; Tozuka, Z.; Ikehara, M.
Tetrahedron Letters, 1981 , vol. 22, # 45 p. 4483 - 4486
反应条件
triethylamine in ethyl acetate
T=0°C;
参考文献
Shealy, Y. Fulmer; Krauth, Charles A.; Struck, Robert F.; Montgomery, John A.
Journal of Medicinal Chemistry, 1983 , vol. 26, # 8 p. 1168 - 1173
反应条件
(i) Et3N, (ii) Al, (iii) AcOH; Multistep reaction;
参考文献
Sih; Heather; Sood; Price; Peruzzotti; Lee
Journal of the American Chemical Society, 1975 , vol. 97, # 4 p. 865 - 874
反应条件
hexamethyl-silane; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in ethylbenzene
T=140°C; 3 h;
参考文献
Kashiwabara, Taigo; Tanaka, Masato
Tetrahedron Letters, 2005 , vol. 46, # 42 p. 7125 - 7128
反应条件
sodium hydrogencarbonate; sodium sulfite in water
T=70 - 80°C; 50 h;
参考文献
Qian, Yu; Shanahan, Charles S.; Doyle, Michael P.
European Journal of Organic Chemistry, 2013 , # 27 p. 6032 - 6037
反应条件
in sodium hydroxide
T=60 - 70°C;
参考文献
Horner, Leopold; Schmitt, Rolf-Erhard
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 189 - 212
参考文献
Leandri et al.
Annali di Chimica (Rome, Italy), 1959 , vol. 49, p. 407,418,421
反应条件
1: NaN3 / acetone; H2O
2: dodecane
View Scheme
参考文献
Abramovitch,R.A. et al.
Journal of Organic Chemistry, 1977 , vol. 42, p. 2920 - 2926
反应条件
4-(N,N-dimethlyamino)pyridine; hydroxylamine hydrochloride in pyridine
T=20°C; 0.0833333 h; Cooling with ice;
参考文献
Aizawa, Kazuyuki; Nakagawa, Hidehiko; Matsuo, Kazuya; Kawai, Kodai; Ieda, Naoya; Suzuki, Takayoshi; Miyata, Naoki
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 8 p. 2340 - 2343
