773837-37-9合成路线 (共 596 条)
反应条件
in neat (no solvent) byproducts: H2; react. of molten NaOH and NaCN at temp. above 500°C in the absence of H2O and O2;;
参考文献
Gmelin Handbook: Na: SVol.4, 2, page 1373 - 1375
反应条件
in not given melting together NaCN and NaOH;;
参考文献
Gmelin Handbook: Na: MVol., 287, page 797 - 799
反应条件
in water byproducts: H2S; addn. of aq. (NH4)2S soln. to ground S; slow addn. of NaCN soln. (half amt.); heating to 90°C; addn. of the rest;; expelling H2S by CO2; concentrating by heating to 135°C; cooling down; crystn. of Na2CO3; concentrating filtrate by heating to 145-150°C;;
参考文献
Gmelin Handbook: Na: SVol.4, 9, page 1387 - 1389
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Pittsburgh Coke and Iron Co.
Patent: US2372119 , 1945 ;
C. A., 1945 , p. 3403
反应条件
tri-tert-butyl phosphine; Pd2(dba)5; zinc in tetrahydrofuran; acetonitrile T=70°C; 2 h;
参考文献
Ushkov, Alexander V.; Grushin, Vladimir V.
Journal of the American Chemical Society, 2011 , vol. 133, # 28 p. 10999 - 11005
反应条件
Eu(II)-DTPA T=20°C; P=760.051 Torr; pH=7.8; Tris buffer;
参考文献
Lee, Chi Chung; Hu, Yilin; Ribbe, Markus W.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 8 p. 1947 - 1949
反应条件
Eu(II)-DTPA T=20°C; P=760.051 Torr; pH=7.8; Tris buffer;
参考文献
Lee, Chi Chung; Hu, Yilin; Ribbe, Markus W.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 8 p. 1947 - 1949
反应条件
ΔnifH MoFe Inert atmosphereEnzymatic reaction;
参考文献
Lee, Chi Chung; Hu, Yilin; Ribbe, Markus W.
Proceedings of the National Academy of Sciences of the United States of America, 2012 , vol. 109, # 18 p. 6922 - 6926
反应条件
in melt Electrolysis; with molten CaF2 (30 percent) LiF (35 percent) and MgF2 at 850°C; carbon anode, liquid Pb cathode, at 7.8 V, 10.8 A/cm2;
参考文献
Gmelin Handbook: F: PerFHalOrg.9, 7, page 50 - 101
反应条件
tri-tert-butyl phosphine; Pd2(dba)5; zinc in tetrahydrofuran; acetonitrile T=70°C; 2 h;
参考文献
Ushkov, Alexander V.; Grushin, Vladimir V.
Journal of the American Chemical Society, 2011 , vol. 133, # 28 p. 10999 - 11005
反应条件
copper (I) cyanide T=20°C;
参考文献
Habibi, Davood; Heydari, Somayyeh; Nasrollahzadeh, Mahmoud
2012 , vol. 36, # 10 p. 573 - 574,2