773837-37-9合成路线 (共 596 条)
反应条件
in neat (no solvent) reduction of CaO with NaCN at 560-750°C in vac.;; no complete reaction;;
参考文献
Gmelin Handbook: Ca: MVol.B2, 15, page 296 - 298
反应条件
in neat (no solvent) React. of STB with NaCN in a BN crucible (1027°C, 15 h).; Extn. with hot water, boiling in HCl, washing (water) and drying (NaCN:Ti=4).;
参考文献
Bamberger; Angelini; Nolan
Journal of the American Ceramic Society, 1989 , vol. 72, # 4 p. 587 - 592
反应条件
in vacuum at 500-750°C;;
参考文献
Gmelin Handbook: Pb: MVol.C1, 32, page 115 - 117
参考文献
Gmelin Handbook: Al: MVol.B1, 7.5.1.1, page 287 - 290
反应条件
nickel oxide in neat (no solvent) byproducts: CO2, CO, N-oxides; warming in mixture with Na3CO3 and NiO to 350°C, react. with O2 or air; Na2CO3 to avoid explosions, absorption of evolded N-oxides in alkaline soln. in form of nitrate, CO is used for heating;;
参考文献
Gmelin Handbook: Na: SVol.1, 18, page 106 - 108
Full Text Show Details
Mentzel, A.
Patent: DE531274 , 1931 ;
C. II, 1931 , p. 3027
反应条件
oxygen byproducts: N2, H2O; react. of molten NaOH and NaCN in the presence of O2 (excess);;
参考文献
Gmelin Handbook: Na: SVol.4, 2, page 1373 - 1375
反应条件
copper (I) cyanide; lithium tert-butylate in 1,4-dioxane; m-xylene T=110°C; 12 h; Inert atmosphere; regioselective reaction;
参考文献
Do, Hien-Quang; Daugulis, Olafs
Organic Letters, 2010 , vol. 12, # 11 p. 2517 - 2519
反应条件
copper (I) cyanide; lithium tert-butylate in 1,4-dioxane; m-xylene T=110°C; 12 h; Inert atmosphere; regioselective reaction;
参考文献
Do, Hien-Quang; Daugulis, Olafs
Organic Letters, 2010 , vol. 12, # 11 p. 2517 - 2519
反应条件
ΔnifH MoFe Inert atmosphereEnzymatic reaction;
参考文献
Lee, Chi Chung; Hu, Yilin; Ribbe, Markus W.
Proceedings of the National Academy of Sciences of the United States of America, 2012 , vol. 109, # 18 p. 6922 - 6926
反应条件
in ethanol; water 16 h; Cooling with ice;
参考文献
Eagon, Scott; Ball-Jones, Nicholas; Haddenham, Dustin; Saavedra, Jaime; Delieto, Cassandra; Buckman, Matthew; Singaram, Bakthan
Tetrahedron Letters, 2010 , vol. 51, # 49 p. 6418 - 6421