773837-37-9合成路线 （共 596 条）
反应条件
sodium tetrahydroborate in methanol; formamide
参考文献
Kwon, Tae Hoon; Yoon, Ik Hwan; Shin, Ji-Sun; Lee, Young Hun; Kwon, Bong Jin; Lee, Kyung-Tae; Lee, Yong Sup
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 9 p. 2571 - 2574
反应条件
Eu(II)-DTPA T=20°C; P=760.051 Torr; pH=7.8; Tris buffer;
参考文献
Lee, Chi Chung; Hu, Yilin; Ribbe, Markus W.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 8 p. 1947 - 1949
反应条件
ΔnifH MoFe Inert atmosphereEnzymatic reaction;
参考文献
Lee, Chi Chung; Hu, Yilin; Ribbe, Markus W.
Proceedings of the National Academy of Sciences of the United States of America, 2012 , vol. 109, # 18 p. 6922 - 6926
反应条件
1: 1-chloro-3-phenoxy-2-propanone With alcohol dehydrogenase from Lactobacillus brevis; NADPH; isopropyl alcohol T=30°C; pH=7.5; 6 h; aq. bufferEnzymatic reaction; 2: sodium cyanide With halohydrin dehalogenase from Mycobacterium sp. GP1 T=30°C; pH=7.5; 18 h; aq. bufferEnzymatic reaction; optical yield given as percent ee;
参考文献
European Journal of Organic Chemistry, , # 14 p. 2293 - 2298
反应条件
copper (I) cyanide; lithium tert-butylate in 1,4-dioxane T=100°C; 12 h; Inert atmosphere; regioselective reaction;
参考文献
Do, Hien-Quang; Daugulis, Olafs
Organic Letters, 2010 , vol. 12, # 11 p. 2517 - 2519
反应条件
in further solvent(s) Kinetics; 298.2 K in Triton X-100;
参考文献
Burgess, John; Patei, Marttand S.
Journal of the Chemical Society, Faraday Transactions, 1993 , vol. 89, # 5 p. 783 - 788
反应条件
byproducts: CO; Heating (1000°C) intimately ground mixt. of starting materials in molar ratio NaCN:BPO4:Na3PO4 = 1:1:1.; SEM anal.;
参考文献
Bamberger; Begun
Journal of the American Ceramic Society, 1986 , vol. 69, # 5 p. c. 95-c. 97
反应条件
byproducts: CO; Heating (1000°C, 17 h, Ar or N2) intimately ground mixt. of starting materials in molar ratio NaCN:BPO4 = 1.; Removal of soluble compd. by washing a fraction of light-colored products with hot (80°C) H2O and then with acetone followed by drying of residues (120°C). XRD and EDX for solids, and Raman spectroscopy for solids and aliquots of aq. ext.;
参考文献
Bamberger; Begun
Journal of the American Ceramic Society, 1986 , vol. 69, # 5 p. c. 95-c. 97
反应条件
byproducts: P, N2, CO; Heating (1000°C, 17 h, Ar or N2) intimately ground mixt. of starting materials in molar ratio NaCN:BPO4 between 1.714 and 2.; Removal of soluble compd. by washing a fraction of light-colored products with hot (80°C) H2O and then with acetone followed by drying of residues (120°C). XRD and EDX for solids, and Raman spectroscopy for solids and aliquots of aq. ext.;
参考文献
Bamberger; Begun
Journal of the American Ceramic Society, 1986 , vol. 69, # 5 p. c. 95-c. 97
反应条件
byproducts: CO, P, N2; Heating (1000°C, 17 h, Ar or N2) intimately ground mixt. of starting materials in molar ratio NaCN:BPO4 between 1.24 and 1.714.; Removal of soluble compd. by washing a fraction of light-colored products with hot (80°C) H2O and then with acetone followed by drying of residues (120°C). XRD and EDX for solids, and Raman spectroscopy for solids and aliquots of aq. ext.;
参考文献
Bamberger; Begun
Journal of the American Ceramic Society, 1986 , vol. 69, # 5 p. c. 95-c. 97
