773837-37-9合成路线 （共 596 条）
反应条件
tri-tert-butyl phosphine; Pd2(dba)5; zinc in tetrahydrofuran; acetonitrile T=70°C; 2 h;
参考文献
Ushkov, Alexander V.; Grushin, Vladimir V.
Journal of the American Chemical Society, 2011 , vol. 133, # 28 p. 10999 - 11005
反应条件
in diethyl ether; water T=20°C;
参考文献
H. LUNDBECK A/S
Patent: US2010/22546 A1, 2010 ;
Location in patent: Page/Page column 17 ;
反应条件
2Na(2+)*O3S2(2-) in water
参考文献
Desai, Nutan H. Palsule; Bairwa, Ranjeet; Kakwani, Manoj; Tawari, Nilesh; Ray; Rajan; Degani, Mariam
Medicinal Chemistry Research, 2013 , vol. 22, # 1 p. 401 - 408
反应条件
C6H18NO3Si(1+)*C7H16Cl3NO5RuSi(1-); dihydrogen peroxide; acetic acid in methanol; water T=20°C; 1.5 h; Reagent/catalyst;
参考文献
Kumar, Subodh; Kumar, Pawan; Jain, Suman L.
RSC Advances, 2013 , vol. 3, # 46 p. 24013 - 24016
反应条件
1: benzaldehyde With DOWER(R)50WX4 in acetonitrile T=20°C; 0.0833333 h; 2: sodium cyanide in acetonitrile T=20°C; 1 h;
参考文献
Sofighaderi, Sargol; Setamdideh, Davood
Oriental Journal of Chemistry, 2013 , vol. 29, # 3 p. 1135 - 1137
反应条件
in ethanol T=85°C; 2 h;
参考文献
MANNKIND CORPORATION; TOLERO PHARMACEUTICALS, INC.; ZENG, Qingping; FARIS, Mary; MOLLARD, Alexis; WARNER, Steven L.; FLYNN, Gary A.
Patent: WO2014/52365 A1, 2014 ;
Location in patent: Page/Page column 302-303 ;
反应条件
in water compds. dissolved in degassed H2O at 80°C, allowed to stand for 1d at 4°C; NaF filtered off, washed with ice-cold EtOH, aq. EtOH mixt. evapd.;
参考文献
Reckeweg, Olaf; Simon, Arndt
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2002 , vol. 57, # 8 p. 895 - 900
反应条件
in neat (no solvent) byproducts: N2; at 550°C, although evolving of N2 but no formation of cyanamide;;
参考文献
Gmelin Handbook: Zn: SVol., 260, page 855 - 857
反应条件
in water (The Chem. of Cyano Complexes of the Transition Elements, Academic Press: London, 1976, p. 287); aq. soln. of NaCN was stirred into aq. soln. ofZn compd.; filtered; washed (water); washed (acetone); dried (vac.);
参考文献
Dance, Ian G.; Dean, Philip A. W.; Fisher, Keith J.; Harris, Hugh H.
Inorganic Chemistry, 2002 , vol. 41, # 13 p. 3560 - 3569
参考文献
Gmelin Handbook: Zn: MVol., 96, page 257 - 259
