773837-37-9合成路线 (共 596 条)
反应条件
in methanol; water Kolbe nitrile synthesis; 1.25 h; Reflux;
参考文献
Pechlivanidis, Zissis; Hopf, Henning; Ernst, Ludger
European Journal of Organic Chemistry, 2009 , # 2 p. 223 - 237
反应条件
1: (E)-1-chlorooctan-2-one With isopropyl alcohol T=30°C; pH=7.5; 4 h; aq. bufferEnzymatic reaction; 2: sodium cyanide With halohydrin dehalogenase from Mycobacterium sp. GP1 T=30°C; pH=7.5; 20 h; aq. bufferEnzymatic reaction; optical yield given as percent ee;
参考文献
European Journal of Organic Chemistry, , # 14 p. 2293 - 2298
反应条件
tri-tert-butyl phosphine; Pd2(dba)5; zinc in tetrahydrofuran; acetonitrile T=70°C; 2 h;
参考文献
Ushkov, Alexander V.; Grushin, Vladimir V.
Journal of the American Chemical Society, 2011 , vol. 133, # 28 p. 10999 - 11005
反应条件
oxygen in water byproducts: NH3; at 37.5°C, 40h, induced by glucose being oxidized in alkaline medium;;
参考文献
Gmelin Handbook: Na: SVol.4, 4, page 1377 - 1379
反应条件
ammonium hydroxide in ethanol; water Bucherer-Lieb reaction; 6 h; Reflux;
参考文献
Naydenova, Emilia D.; Todorov, Petar T.; Troev, Kolio D.
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 7 p. 1315 - 1320
反应条件
calcium dihydride; tri-tert-butyl phosphine; Pd2(dba)5 in tetrahydrofuran; acetonitrile T=70°C; 2 h;
参考文献
Ushkov, Alexander V.; Grushin, Vladimir V.
Journal of the American Chemical Society, 2011 , vol. 133, # 28 p. 10999 - 11005
反应条件
in water; N,N-dimethyl-formamide T=20°C; chemoselective reaction;
参考文献
Patil, Shivaraj P.; Kanawade, Shrikant B.; Shinde, Madhukar P.; Toche, Raghunath B.
Indian Journal of Heterocyclic Chemistry, 2011 , vol. 21, # 1 p. 33 - 36
反应条件
in ethanol; water T=20°C;
参考文献
Indian Journal of Heterocyclic Chemistry, , vol. 21, # 1 p. 33 - 36
反应条件
in water Kinetics; at 25, 69.84 and 90.00 °C;;
参考文献
Gmelin Handbook: Na: SVol.4, 4, page 1377 - 1379
反应条件
in methanol Kinetics;
参考文献
Gmelin Handbook: C: MVol.D1, 3.4, page 31 - 44