773837-37-9合成路线 （共 596 条）
反应条件
polyethylene glycol-silica hybrid nanocomposite in water T=90°C; Green chemistry; Overall yield = 90 percent; regioselective reaction;
参考文献
Kiasat, Ali Reza; Nazari, Simin; Davarpanah, Jamal
Comptes Rendus Chimie, 2014 , vol. 17, # 2 p. 124 - 130
反应条件
water in ethanol 24 h; Reflux;
参考文献
Schrittwieser, Joerg H.; Lavandera, Ivan; Seisser, Birgit; Mautner, Barbara; Kroutil, Wolfgang
European Journal of Organic Chemistry, 2009 , # 14 p. 2293 - 2298
反应条件
grobacterium radiobacter strain AD1 gene halohydrin dehalogenase mutant in aq. buffer T=30°C; pH=7; 18 h; Enzymatic reaction; stereoselective reaction;
参考文献
Chen, Shao-Yun; Yang, Chen-Xi; Wu, Jian-Ping; Xu, Gang; Yang, Li-Rong
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 16 p. 3179 - 3190
反应条件
in methanol; water T=80 - 90°C; Reflux; ConcentrationTimeTemperature;
参考文献
HIKAL LIMITED; YERANDE, Swapnil, Gulabrao; THAKUR, Rajesh, Mataprasad; SHARMA, Sundarakrishna, S.; GANGOPADHYAY, Ashok, Kumar; RUPP, Helmut; KUBAVAT, Hitesh; NAGARAJAN, Kuppuswamy; SELVAN, Arul; NUNNA, Rambabu; JALAJAKSHI, Vivekananda, Induharappa
Patent: WO2013/190357 A1, 2013 ;
Location in patent: Page/Page column 16-17 ;
反应条件
ammonium acetate in methanol T=65 - 95°C;
参考文献
HIKAL LIMITED; YERANDE, Swapnil, Gulabrao; THAKUR, Rajesh, Mataprasad; SHARMA, Sundarakrishna, S.; GANGOPADHYAY, Ashok, Kumar; RUPP, Helmut; KUBAVAT, Hitesh; NAGARAJAN, Kuppuswamy; SELVAN, Arul; NUNNA, Rambabu; JALAJAKSHI, Vivekananda, Induharappa
Patent: WO2013/190357 A1, 2013 ;
Location in patent: Page/Page column 18 ;
反应条件
sodium hydroxide in water-d2 a mixt. of NaCN, NaOH and D2O was refluxed for 2 wk; distd., the residue was dissolved in H2O, HCl to pH 8.0 was added;
参考文献
Wong; Whitesides
Journal of the American Chemical Society, 1983 , vol. 105, # 15 p. 5012 - 5014
反应条件
in water-d2 byproducts: ND3; heating educts in closed pyrex glass tube at 180°C, 3h;; separation of ND3; evapn. at 110°C; dissoln. in H2O; treating with active coal;;
参考文献
Gmelin Handbook: Na: SVol.4, 20, page 1410 - 1412
反应条件
in ethanol 4 h; Reflux;
参考文献
Landge, Kamalkishor P.; Jang, Keun Sam; Lee, Sang Yeul; Chi, Dae Yoon
Journal of Organic Chemistry, 2012 , vol. 77, # 13 p. 5705 - 5713
反应条件
in dimethyl sulfoxide T=110°C; 5 h;
参考文献
Meroni, Giuseppe; Ciana, Paolo; Maggi, Adriana; Santaniello, Enzo
Synlett, 2009 , # 16 p. 2682 - 2684
反应条件
1: 2-amino-6-methoxy-benzthiazole With sulfuric acid; sodium nitrite in acetic acid Sandmeyer reaction; 2: sodium cyanide; copper (I) cyanide With sodium hydrogencarbonate; acetic acid in water Sandmeyer reaction; Cooling with ice;
参考文献
Zhang, Bin; Li, Jianli; Chen, Wei; Wang, Yunxia; Shi, Zhen
Chinese Journal of Chemistry, 2010 , vol. 28, # 1 p. 111 - 114
