6-乙酰基-1,2,3,4-四氢萘合成路线 （共 49 条）
反应条件
aluminium trichloride; benzene
参考文献
Journal of Organic Chemistry, , vol. 23, p. 994
Chemische Berichte, , vol. 90, p. 2949
Doklady Akademii Nauk SSSR, , vol. 83, p. 235,237
Chem.Abstr., 1053 4321
反应条件
1: 90 percent / I2, P(red) / toluene / 8 h / Heating 2: 67 percent / KOH / methanol / 4 h / Heating 3: 76 percent / toluene / 12 h / 60 °C 4: 93 percent / 1,5-diazabicyclo<4.3.0>non-5-ene / toluene / 24 h / Ambient temperature 5: 66 percent / DDQ / CH2Cl2 / 4 h / 0 °C View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 112, # 4 p. 237 - 246
反应条件
1: 67 percent / KOH / methanol / 4 h / Heating 2: 76 percent / toluene / 12 h / 60 °C 3: 93 percent / 1,5-diazabicyclo<4.3.0>non-5-ene / toluene / 24 h / Ambient temperature 4: 66 percent / DDQ / CH2Cl2 / 4 h / 0 °C View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 112, # 4 p. 237 - 246
反应条件
1: 93 percent / 1,5-diazabicyclo<4.3.0>non-5-ene / toluene / 24 h / Ambient temperature 2: 66 percent / DDQ / CH2Cl2 / 4 h / 0 °C View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 112, # 4 p. 237 - 246
反应条件
1: 55 percent / LiAlH4 / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) r. t. overnight 2: 90 percent / I2, P(red) / toluene / 8 h / Heating 3: 67 percent / KOH / methanol / 4 h / Heating 4: 76 percent / toluene / 12 h / 60 °C 5: 93 percent / 1,5-diazabicyclo<4.3.0>non-5-ene / toluene / 24 h / Ambient temperature 6: 66 percent / DDQ / CH2Cl2 / 4 h / 0 °C View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 112, # 4 p. 237 - 246
反应条件
1: 76 percent / toluene / 12 h / 60 °C 2: 93 percent / 1,5-diazabicyclo<4.3.0>non-5-ene / toluene / 24 h / Ambient temperature 3: 66 percent / DDQ / CH2Cl2 / 4 h / 0 °C View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 112, # 4 p. 237 - 246
反应条件
1: 31 percent / EDA, Li / tetrahydrofuran / 1 h / 20 - 25 °C 2: 80 percent / Jones reagent / 0.02 h / 0 °C View Scheme
参考文献
Polish Journal of Chemistry, , vol. 54, # 3 p. 453 - 459
反应条件
carbon disulfide; aluminium trichloride
参考文献
Chemische Berichte, , vol. 35, p. 2511
参考文献
Indian Journal of Chemistry, , vol. 7, p. 105 - 110
反应条件
aluminium trichloride; nitrobenzene
