in 1,4-dioxane-d8
T=101°C; 20 h; Inert atmosphere;
参考文献
Van Kalkeren, Henri A.; Bruins, Jorick J.; Rutjes, Floris P. J. T.; Van Delft, Floris L.
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 8 p. 1417 - 1421
in benzene-d6
(Ar); std. Schlenk technique; Si compd. (3 equiv.) was added to soln. ofPt complex (1 equiv.) in C6D6 at room temp. in NMR tube; reacted for 46 h; NMR monitoring;