反应条件
1.1: sodium azide / N,N-dimethyl-formamide / 16 h / 20 °C 2.1: potassium tert-butylate / tert-butyl alcohol / 0.25 h / 30 °C 2.2: 16 h / 30 °C 3.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C View Scheme
参考文献
Devigny, Christian; Perez-Balderas, Francisco; Hoogeland, Bastiaan; Cuboni, Serena; Wachtel, Rudolf; Mauch, Christoph P.; Webb, Katharine J.; Deussing, Jan M.; Hausch, Felix
Journal of the American Chemical Society, 2011 , vol. 133, # 23 p. 8927 - 8933