in further solvent(s) Kinetics; soln. of I2 in tributylphosphate (TBP) quickly added to soln. of KMnO4 in TBP at 20°C and stirred (magnetic stirrer); reaction stopped by quickly vacuum-filtering the mixt. in Mohr's salt and octane, solid products remain in filter;
参考文献
Radiokhimiya, , vol. 32, p. 495 - 499
Radiokhimiya, , vol. 32 - 5, p. 73 - 77
in neat (no solvent) heating dry equivalent mixture of KClO3 and KI to temp. between melting point of KClO3 and decomposition temp. of KIO3 in stream of O2; cooling down;; trituration and washing with cold H2O, fractionated crystallization;;
参考文献
I: MVol.2, 121, page 506 - 508
Nouvelles recherches sur les lois des proportions chimiques, sur les poids atomiques et leurs rapports mutuels, Bruxelles 1865, S. 113
in neat (no solvent) Kinetics; reaction with KOH in the absence or the presence of solvent;; yield depending on time and temp.;;
参考文献
Banus, J.; Emeleus, H. J.; Haszeldine, R. N.
Journal of the Chemical Society, 1951 , p. 60 - 64
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Gmelin Handbook: C: MVol.D2, 4.2.4.4.7, page 322 - 323
