2,3-二氢-4(1H)-菲酮合成路线 （共 49 条）
反应条件
1: With boron trifluoride diethyl etherate; [Pd(CH3CN)4](BF4)2 in various solvent(s) T=20°C; Friedel-Crafts cyclization; 2160 h; 2: With phosphate buffer in various solvent(s) pH=7; Further stages.;
参考文献
Organic Letters, , vol. 9, # 22 p. 4639 - 4642
反应条件
methanesulfonic acid T=90°C; 1 h;
参考文献
Wiznycia, Alexander V.; Desper, John; Levy, Christopher J.
Chemical Communications, 2005 , # 37 p. 4693 - 4695
反应条件
1: With boron trifluoride diethyl etherate; [Pd(CH3CN)4](BF4)2 in various solvent(s) T=20°C; Friedel-Crafts cyclization; 0.666667 h; 2: With phosphate buffer in various solvent(s) pH=7; Further stages.;
参考文献
Organic Letters, , vol. 9, # 22 p. 4639 - 4642
反应条件
1: With [Pd(MeCN)2Cl2](BF4)2 in various solvent(s) T=20°C; Friedel-Crafts cyclization; 3 h; 2: With phosphate buffer in various solvent(s) pH=7; Further stages.;
参考文献
Yokota, Misaki; Fujita, Daishi; Ichikawa, Junji
Organic Letters, 2007 , vol. 9, # 22 p. 4639 - 4642
反应条件
1: 91 percent / H2NNH2*H2O / bis-(2-hydroxy-ethyl) ether / 16 h / 195 °C 2: 96 percent / CH3SO3H / 1 h / 90 °C View Scheme
参考文献
Chemical Communications, , # 37 p. 4693 - 4695
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 5 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 59, # 25 p. 7876 - 7888
参考文献
Journal of the American Chemical Society, , vol. 68, p. 2580,2583
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 1 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 59, # 25 p. 7876 - 7888
反应条件
2: H2NNH2*H2O, KOH / bis-(2-hydroxy-ethyl) ether 3: 1.) PCl5, 2.) SnCl4 / 2.) benzene View Scheme
参考文献
Journal of the American Chemical Society, , vol. 119, # 31 p. 7241 - 7248
反应条件
1: H2 / 10percent Pd/C / ethanol / 775.7 Torr 2: PCl5 3: SnCl4 View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 39, # 15 p. 3001 - 3013
